Influence of the synthesis conditions of boron carbide on its structural parameters View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2016-09

AUTHORS

D. Yu. Kovalev, V. I. Ponomarev, S. V. Konovalikhin, V. I. Vershinnikov, I. D. Kovalev

ABSTRACT

Boron carbide is prepared by self-propagating high-temperature synthesis (SHS) in a composition range from 5 to 30 at % carbon. The introduction of an inert (MgO) and active (Mg(ClO4)2) additives into the reaction mixture leads to a variation in process parameters such as the temperature and combustion rate. It is established that the unit cell metrics of boron carbide substantially vary depending on the synthesis conditions. The degree of the effect of the SHS mode on the crystal structure rises with an increase in the carbon fraction in the boron carbide structure. This regularity is associated with the ordering diversity of carbon atoms in nonstoichiometric boron carbide. No influence of the synthesis conditions on the unit cell parameters is observed for stoichiometric boron carbide, which is associated with the structure saturation with carbon. It is shown that the variation in the combustion temperature during SHS of boron carbide of the same composition leads to the variability of the structural parameters, thus reflecting the influence of the synthesis conditions on the material crystal structure. More... »

PAGES

604-609

References to SciGraph publications

  • 2009-02. Carbon in boron carbide: The crystal structure of B11.4C3.6 in RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
  • 2013-05. Ordering of carbon atoms in boron carbide structure in CRYSTALLOGRAPHY REPORTS
  • 2013-07. SHS of single crystals in the B-C-Mg system: Crystal structure of new modification of B25C4Mg1.42 = [B12]2[CBC][C2]Mg1.42 in INTERNATIONAL JOURNAL OF SELF-PROPAGATING HIGH-TEMPERATURE SYNTHESIS
  • 2012-04. SHS-produced boron carbide: Some special features of crystal structure in INTERNATIONAL JOURNAL OF SELF-PROPAGATING HIGH-TEMPERATURE SYNTHESIS
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    http://scigraph.springernature.com/pub.10.3103/s1067821216060092

    DOI

    http://dx.doi.org/10.3103/s1067821216060092

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    https://app.dimensions.ai/details/publication/pub.1017636048


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