Crystal structure of dense pseudo-cubic boron allotrope, pc-B52, by powder X-ray diffraction View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2013-02

AUTHORS

O. O. Kurakevych, V. L. Solozhenko

ABSTRACT

During past years, a number of reports have been published on synthesis of tetragonal allotrope of boron, t-B52 phase. However, no unambiguous characterization of the crystal structure has been performed to the present time, while remarkable variation of the a/c lattice-parameter ratio raises strong doubts about its uniqueness. Here the Rietveld refinement of the crystal structure of the high pressure-high temperature boron phase synthesized by a direct solid-state transformation of rhombohedral β-B106 at 20 GPa and 2500 K has been reported for the first time. Although this boron allotrope belongs to the t-B52 type, its structure can be considered as pseudo-cubic with the a/c ratio of . More... »

PAGES

60-63

Identifiers

URI

http://scigraph.springernature.com/pub.10.3103/s1063457613010085

DOI

http://dx.doi.org/10.3103/s1063457613010085

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1047806430


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