Pd/Fiber glass and Pd/5% γ-Al2O3/Fiber glass catalysts by surface self-propagating thermal synthesis View Full Text


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Article Info

DATE

2012-04

AUTHORS

O. O. Mironenko, N. B. Shitova, Y. S. Kotolevich, M. R. Sharafutdinov, N. O. Struikhina, N. S. Smirnova, D. I. Kochubey, O. V. Protasova, M. V. Trenikhin, O. A. Stonkus, V. I. Zaikovskii, V. B. Goncharov, P. G. Tsyrul’nikov

ABSTRACT

The technique of Surface Self-propagating Thermal Synthesis (SSTS) was used to prepare Pd/γ-Al2O3/fiber glass (FG) catalysts for selective liquid-phase hydrogenation of acetylene in the presence of CO. The results of XRD SR analysis (in synchrotron radiation) in combination with the technique of arrested combustion shed new light on the dynamic of phase transformations in the systems under study and variation in the size of diffraction-active crystallites. The catalytic performance of synthesized catalysts was found to be close to that of similar conventionally prepared catalysts. The EXAFS and TEM data afforded to estimate the variation in relative amounts of Pd0 and PdO in synthesized catalysts. In the course of selective hydrogenation, PdO rapidly (<15 min) reduced to Pd0. More... »

PAGES

139-145

Identifiers

URI

http://scigraph.springernature.com/pub.10.3103/s1061386212020082

DOI

http://dx.doi.org/10.3103/s1061386212020082

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1010966179


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