Influence of thermal treatment on the morphology of zinc oxide NPs synthesized by green method View Full Text


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Article Info

DATE

2022-04-19

AUTHORS

Danish Majeed, Asad A. Zaidi, Muhammad Nihal Naseer, Muhammad Asif

ABSTRACT

Present research paper focuses on the morphological changes that occur in zinc oxide NPs due to thermal treatment that are synthesized using green synthesis technique. The method selected for NPs synthesis incorporates the utilization of zinc nitrate salt and aloe vera extract. X-ray diffraction technique is utilized to confirm the chemical structure of the as-synthesized material. Size and morphology studies were carried out by changing reaction and calcination temperatures. Reaction temperatures were varied by 4° i.e., 64 °C, 68 °C and 72 °C, while calcination temperature variations were of hundred degrees, i.e., 470 °C, 570 °C and 670 °C. Scanning electron microscopy of samples at different reactions and calcination temperatures was also conducted. Particle size is determined using Debye Scherer formula. UV–Visible Spectroscopy was also opted to confirm zinc oxide at a wavelength of 368 nm. Results show that with increased calcination temperature there is a sharp morphological change from plates to hexagonal rods and from rods to spherical particles.Graphical abstract More... »

PAGES

420-426

Identifiers

URI

http://scigraph.springernature.com/pub.10.1557/s43580-022-00279-2

DOI

http://dx.doi.org/10.1557/s43580-022-00279-2

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https://app.dimensions.ai/details/publication/pub.1147221579


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