Simultaneous Isolation and Purification of Mollugin and Two Anthraquinones from Rubia cordifolia by HSCCC View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2008-07

AUTHORS

Rui Liu, Yanbin Lu, Tianxing Wu, Yuanjiang Pan

ABSTRACT

A preparative high-speed countercurrent chromatography (HSCCC) method for isolation and purification of three bioactive components, tectoquinone; 1-hydroxy-2-methylanthraquinone and mollugin from the Chinese medicinal plant Rubia cordifolia was successfully established. With a two-phase solvent system composed of light petroleum/ethanol/diethyl ether/water (5:4:3:1, v/v), 10 mg tectoquinone, 19 mg 1-hydroxy-2-methylanthraquinone and 16 mg mollugin were obtained from 100 mg of the crude petroleum extract in a one-step separation at a purity of 98.8, 95.8 and 98.3%, respectively. The structures of mollugin and anthraquinones were identified by 1H NMR and 13C NMR. More... »

PAGES

95-99

Journal

TITLE

Chromatographia

ISSUE

1-2

VOLUME

68

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1365/s10337-008-0629-z

DOI

http://dx.doi.org/10.1365/s10337-008-0629-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1003562916


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