Graft Copolymers Having Hydrophobic Backbone and Hydrophilic Branches XXXIV. Fabrication and Control of Honeycomb Structure Prepared from Amphiphilic Graft Copolymers View Full Text


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Article Info

DATE

2001

AUTHORS

Ken-ichiro Hiwatari, Takeshi Serizawa, Fusako Seto, Akio Kishida, Yoichiro Muraoka, Mitsuru Akashi

ABSTRACT

Well-controlled polymeric honeycomb structures were made from graft copolymer prepared by free radical polymerization of a poly(ethylene glycol) (PEG) macromonomer and styrene with N,N-azobisisobutyronitrile (AIBN) as radical initiator in ethanol/water (4/1, v/v) solvent. Macroporous polymeric films were formed when chloroform solution of the freeze-dried nanospheres was dip-coated under controlled conditions of humidity and while controlling the composition of the graft copolymer and the type of substrate. Highly-ordered and monodispersed pores were formed on polymeric film surfaces from the graft copolymer (St/(PEG macromonomer) ratio = 105/1, mol/mol) under controlled conditions (humidity, 70% (RH); pulling up speed, 500 cm min-1). Control of humidity during the dip-coat process was essential for formation of the ordered porous structure. Macroporous structures were formed possibly by condensed water-droplets as templates. The formation of pores on the film was dependent on concentration of the solution. When dip-coated in a 3 (w/v) % solution, the pores did not penetrate the substrate. In contrast, pores penetrated it from a 1 (w/v)% solution. Graft copolymers formed a unique structure under controlled regulatory conditions. More... »

PAGES

669

Identifiers

URI

http://scigraph.springernature.com/pub.10.1295/polymj.33.669

DOI

http://dx.doi.org/10.1295/polymj.33.669

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https://app.dimensions.ai/details/publication/pub.1026616362


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