Synthesis and Characterization of Nanoscale Tungsten Particles with Hollow Superstructure Using Spray Drying Combined with Calcination Process View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2019-12

AUTHORS

Panchao Zhao, Wei Yi, Qigao Cao, Bosheng Zhang, Kunkun Chen, Rui Dang, Jialin Chen

ABSTRACT

Nanoscale tungsten (W) powder is used in some special materials. In this study, a hollow superstructure W powder consisting of nanoparticles was synthesized by spray drying combined with two-step calcination from commercial (NH4)6W7O24·6H2O. The high-pressure gas (HPG) was the significant factor in spray drying process, which affect the BET surface area and average particles size of the spray-dried powders. The detailed influences of calcined steps and calcination temperature in the microstructure and average particles size of final W particles were investigated. The size distribution of as-synthesized nanoscale W particles with hollow superstructure was from 40 to 200 nm, and the average size was about 100 nm. The as-synthesized W powder shows good sintering properties. It should be noted that the powder technology in this study can be used to synthesize other powders with high-performance requirements. . More... »

PAGES

68

Identifiers

URI

http://scigraph.springernature.com/pub.10.1186/s11671-019-2904-3

DOI

http://dx.doi.org/10.1186/s11671-019-2904-3

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1112390063

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30806833


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