Syntheses, characterizations and thermal analyses of four novel unsymmetrical β-diketiminates View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2013-12

AUTHORS

Siddappa A Patil, Phillip A Medina, Joseph W Ziller, Bradley D Fahlman

ABSTRACT

Four novel unsymmetrical β-diketiminates 2-(2,6-diisopropylphenyl)amino-4-(phenyl)imino-2-pentene (4a), 2-(2,6-diisopropylphenyl)amino-4-(4-methylphenyl)imino-2-pentene (4b), 2-(2,6-diisopropylphenyl)amino-4-(4-methoxyphenyl)imino-2-pentene (4c) and 2-(2,6-diisopropylphenyl)amino-4-(4-chlorophenyl)imino-2-pentene (4d) were synthesized with a 77-84% yield, and were characterized by spectroscopic methods ((1)H NMR, (13)C NMR, IR and mass spectrometry), elemental analysis, and X-ray single-crystal diffraction, respectively. Spectroscopic and X-ray single-crystal diffraction analyses determined the structures of the four β-diketiminates. While thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) showed two distinct endothermic peaks for each β-diketiminate at temperatures of 92.55°C and 221.50°C (4a), 93.51°C and 238.82°C (4b), 109.60°C and 329.22°C (4c), 115.43°C and 243.25°C (4d), respectively, corresponding to their melting and boiling points. More... »

PAGES

32

Identifiers

URI

http://scigraph.springernature.com/pub.10.1186/2193-1801-2-32

DOI

http://dx.doi.org/10.1186/2193-1801-2-32

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https://app.dimensions.ai/details/publication/pub.1029417314

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/23525855


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