Radical ions from and spin adducts to 1,2-dimethyl-3,4-bis[(2,4,6-tri-tert-butylphenyl) phosphinidene]-1-cyclobutene View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-09

AUTHORS

Angelo Alberti, Massimo Benaglia, Maurizio Guerra, Dante Macciantelli

ABSTRACT

The radical cation and anion of the title compound were obtained either by treatment with mercury trifluorocatetate in trifluoroacetic acid or by reduction with potassium in tetrahydrofurane. For both species the ESR spectra indicated magnetic non-equivalence of the two phosphorus atoms, as well as of the two methyl groups. Spectra attributed to the corresponding spin adducts were also observed when reacting the title compound with in situ-generated alkoxyl and thiyl radicals. MO calculations carried out for both the ionic radicals and the neutral spin adducts led to questioning the actual nature of some of the latter species. More... »

PAGES

725-737

Identifiers

URI

http://scigraph.springernature.com/pub.10.1163/156856707782169363

DOI

http://dx.doi.org/10.1163/156856707782169363

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1012841414


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