Hard X-ray photoemission study of the Fabre salts (TMTTF)2X (X = SbF6 and PF6) View Full Text


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Article Info

DATE

2014-11-03

AUTHORS

Katerina Medjanik, Mariano de Souza, Dmytro Kutnyakhov, Andrei Gloskovskii, Jens Müller, Michael Lang, Jean-Paul Pouget, Pascale Foury-Leylekian, Alec Moradpour, Hans-Joachim Elmers, Gerd Schönhense

ABSTRACT

Core-level photoemission spectra of the Fabre salts with X = SbF6 and PF6 were taken using hard X-rays from PETRA III, Hamburg. In these salts TMTTF layers show a significant stack dimerization with a charge transfer of 1e per dimer to the anion SbF6 or PF6. At room temperature and slightly below the core-level spectra exhibit single lines, characteristic for a well-screened metallic state. At reduced temperatures progressive charge localization sets in, followed by a 2nd order phase transition into a charge-ordered ground state. In both salts groups of new core-level signals occur, shifted towards lower kinetic energies. This is indicative of a reduced transverse-conductivity across the anion layers, visible as layer-dependent charge depletion for both samples. The surface potential was traced via shifts of core-level signals of an adsorbate. A well-defined potential could be established by a conducting cap layer of 5 nm aluminum which appears “transparent” due to the large probing depth of HAXPES (8–10 nm). At the transition into the charge-ordered phase the fluorine 1s line of (TMTTF)2SbF6 shifts by 2.8 eV to higher binding energy. This is a spectroscopic fingerprint of the loss of inversion symmetry accompanied by a cooperative shift of the SbF6 anions towards the more positively charged TMTTF donors. This shift does not occur for the X = PF6 compound, most likely due to smaller charge disproportion or due to the presence of charge disorder. More... »

PAGES

256

References to SciGraph publications

  • 2004. Organic Superconductors in THE PHYSICS OF SUPERCONDUCTORS
  • 2006-02. Neutron-Scattering Evidence for a Spin-Peierls Ground State in (TMTTF)2PF6 in JOURNAL OF LOW TEMPERATURE PHYSICS
  • 2007-05-04. Ordering phenomena in quasi-one-dimensional organic conductors in THE SCIENCE OF NATURE
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    http://scigraph.springernature.com/pub.10.1140/epjb/e2014-50499-y

    DOI

    http://dx.doi.org/10.1140/epjb/e2014-50499-y

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