Low-temperature synthesis of micron nitride powders of the Fe-N system View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-03

AUTHORS

E. P. Kovalev, M. I. Alymov, A. B. Ankudinov, A. G. Gnedovets, V. A. Zelenskii

ABSTRACT

The practical possibility of synthesizing micron-size corrosion-resistant powder materials based on lower and higher nitrides of the Fe-N system in the form of both a bulk composition and a “core-shell” system was implemented at relatively low temperatures. Information on the elemental and chemical composition of iron nitrides was obtained using the methods of Auger electron spectroscopy and X-ray quantitative analysis. Fe3N and Fe4N phases were identified in the volume of microcrystals in the form of compositions with unreacted α-Fe without foreign impurities in the temperature range of 300–350°C. The highest mass concentration of the Fe4N phase was observed at 350°C and a nitriding time of 60 min (α-Fe, 14.70%; Fe3N, 24.50%; and Fe4N, 60.80%). Porous nanocoatings were synthesized on the surfaces of carbonyl iron microparticles at 165°C and a synthesis time of 420 min. This nanocoating has a thickness of ∼10–15 nm and, in the first approximation, corresponds to the ∼Fe15.7N2 compound. More... »

PAGES

168-172

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s2075113314020105

DOI

http://dx.doi.org/10.1134/s2075113314020105

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1031168821


Indexing Status Check whether this publication has been indexed by Scopus and Web Of Science using the SN Indexing Status Tool
Incoming Citations Browse incoming citations for this publication using opencitations.net

JSON-LD is the canonical representation for SciGraph data.

TIP: You can open this SciGraph record using an external JSON-LD service: JSON-LD Playground Google SDTT

[
  {
    "@context": "https://springernature.github.io/scigraph/jsonld/sgcontext.json", 
    "about": [
      {
        "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/0306", 
        "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
        "name": "Physical Chemistry (incl. Structural)", 
        "type": "DefinedTerm"
      }, 
      {
        "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/03", 
        "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
        "name": "Chemical Sciences", 
        "type": "DefinedTerm"
      }
    ], 
    "author": [
      {
        "affiliation": {
          "alternateName": "Russian Academy of Sciences", 
          "id": "https://www.grid.ac/institutes/grid.4886.2", 
          "name": [
            "Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninskii pr. 49, 119991, Moscow, Russia"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Kovalev", 
        "givenName": "E. P.", 
        "id": "sg:person.012234246102.87", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.012234246102.87"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Russian Academy of Sciences", 
          "id": "https://www.grid.ac/institutes/grid.4886.2", 
          "name": [
            "Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninskii pr. 49, 119991, Moscow, Russia"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Alymov", 
        "givenName": "M. I.", 
        "id": "sg:person.015657347013.51", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.015657347013.51"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Russian Academy of Sciences", 
          "id": "https://www.grid.ac/institutes/grid.4886.2", 
          "name": [
            "Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninskii pr. 49, 119991, Moscow, Russia"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Ankudinov", 
        "givenName": "A. B.", 
        "id": "sg:person.013524315623.89", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.013524315623.89"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Russian Academy of Sciences", 
          "id": "https://www.grid.ac/institutes/grid.4886.2", 
          "name": [
            "Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninskii pr. 49, 119991, Moscow, Russia"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Gnedovets", 
        "givenName": "A. G.", 
        "id": "sg:person.015550453605.21", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.015550453605.21"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Russian Academy of Sciences", 
          "id": "https://www.grid.ac/institutes/grid.4886.2", 
          "name": [
            "Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninskii pr. 49, 119991, Moscow, Russia"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Zelenskii", 
        "givenName": "V. A.", 
        "id": "sg:person.011344617213.59", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.011344617213.59"
        ], 
        "type": "Person"
      }
    ], 
    "citation": [
      {
        "id": "https://doi.org/10.1016/j.materresbull.2008.02.008", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1001050951"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/j.jallcom.2005.12.134", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1003695195"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1088/0953-8984/6/4/001", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1008085971"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/s0304-8853(99)00429-1", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1010306878"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.2320/matertrans.maw201023", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1019102700"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1002/bbpc.19300360711", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1027289743"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/s0304-8853(99)00536-3", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1027892221"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1098/rspa.1951.0155", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1043031373"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/j.actamat.2007.08.020", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1049627660"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1088/1367-2630/12/6/063032", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1059135073"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1088/1367-2630/12/6/063032", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1059135073"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1103/physrevb.80.024202", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1060629627"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1103/physrevb.80.024202", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1060629627"
        ], 
        "type": "CreativeWork"
      }
    ], 
    "datePublished": "2014-03", 
    "datePublishedReg": "2014-03-01", 
    "description": "The practical possibility of synthesizing micron-size corrosion-resistant powder materials based on lower and higher nitrides of the Fe-N system in the form of both a bulk composition and a \u201ccore-shell\u201d system was implemented at relatively low temperatures. Information on the elemental and chemical composition of iron nitrides was obtained using the methods of Auger electron spectroscopy and X-ray quantitative analysis. Fe3N and Fe4N phases were identified in the volume of microcrystals in the form of compositions with unreacted \u03b1-Fe without foreign impurities in the temperature range of 300\u2013350\u00b0C. The highest mass concentration of the Fe4N phase was observed at 350\u00b0C and a nitriding time of 60 min (\u03b1-Fe, 14.70%; Fe3N, 24.50%; and Fe4N, 60.80%). Porous nanocoatings were synthesized on the surfaces of carbonyl iron microparticles at 165\u00b0C and a synthesis time of 420 min. This nanocoating has a thickness of \u223c10\u201315 nm and, in the first approximation, corresponds to the \u223cFe15.7N2 compound.", 
    "genre": "research_article", 
    "id": "sg:pub.10.1134/s2075113314020105", 
    "inLanguage": [
      "en"
    ], 
    "isAccessibleForFree": false, 
    "isPartOf": [
      {
        "id": "sg:journal.1135943", 
        "issn": [
          "2075-1133", 
          "2075-115X"
        ], 
        "name": "Inorganic Materials: Applied Research", 
        "type": "Periodical"
      }, 
      {
        "issueNumber": "2", 
        "type": "PublicationIssue"
      }, 
      {
        "type": "PublicationVolume", 
        "volumeNumber": "5"
      }
    ], 
    "name": "Low-temperature synthesis of micron nitride powders of the Fe-N system", 
    "pagination": "168-172", 
    "productId": [
      {
        "name": "readcube_id", 
        "type": "PropertyValue", 
        "value": [
          "947c1cbd6d22a259602872f42dac51ddf1fc5076199704672c3cab621e2da4a2"
        ]
      }, 
      {
        "name": "doi", 
        "type": "PropertyValue", 
        "value": [
          "10.1134/s2075113314020105"
        ]
      }, 
      {
        "name": "dimensions_id", 
        "type": "PropertyValue", 
        "value": [
          "pub.1031168821"
        ]
      }
    ], 
    "sameAs": [
      "https://doi.org/10.1134/s2075113314020105", 
      "https://app.dimensions.ai/details/publication/pub.1031168821"
    ], 
    "sdDataset": "articles", 
    "sdDatePublished": "2019-04-10T16:47", 
    "sdLicense": "https://scigraph.springernature.com/explorer/license/", 
    "sdPublisher": {
      "name": "Springer Nature - SN SciGraph project", 
      "type": "Organization"
    }, 
    "sdSource": "s3://com-uberresearch-data-dimensions-target-20181106-alternative/cleanup/v134/2549eaecd7973599484d7c17b260dba0a4ecb94b/merge/v9/a6c9fde33151104705d4d7ff012ea9563521a3ce/jats-lookup/v90/0000000001_0000000264/records_8669_00000537.jsonl", 
    "type": "ScholarlyArticle", 
    "url": "http://link.springer.com/10.1134%2FS2075113314020105"
  }
]
 

Download the RDF metadata as:  json-ld nt turtle xml License info

HOW TO GET THIS DATA PROGRAMMATICALLY:

JSON-LD is a popular format for linked data which is fully compatible with JSON.

curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/pub.10.1134/s2075113314020105'

N-Triples is a line-based linked data format ideal for batch operations.

curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/pub.10.1134/s2075113314020105'

Turtle is a human-readable linked data format.

curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/pub.10.1134/s2075113314020105'

RDF/XML is a standard XML format for linked data.

curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/pub.10.1134/s2075113314020105'


 

This table displays all metadata directly associated to this object as RDF triples.

122 TRIPLES      21 PREDICATES      38 URIs      19 LITERALS      7 BLANK NODES

Subject Predicate Object
1 sg:pub.10.1134/s2075113314020105 schema:about anzsrc-for:03
2 anzsrc-for:0306
3 schema:author Nd06dc04b556a4d1ea3951a57ca89b54f
4 schema:citation https://doi.org/10.1002/bbpc.19300360711
5 https://doi.org/10.1016/j.actamat.2007.08.020
6 https://doi.org/10.1016/j.jallcom.2005.12.134
7 https://doi.org/10.1016/j.materresbull.2008.02.008
8 https://doi.org/10.1016/s0304-8853(99)00429-1
9 https://doi.org/10.1016/s0304-8853(99)00536-3
10 https://doi.org/10.1088/0953-8984/6/4/001
11 https://doi.org/10.1088/1367-2630/12/6/063032
12 https://doi.org/10.1098/rspa.1951.0155
13 https://doi.org/10.1103/physrevb.80.024202
14 https://doi.org/10.2320/matertrans.maw201023
15 schema:datePublished 2014-03
16 schema:datePublishedReg 2014-03-01
17 schema:description The practical possibility of synthesizing micron-size corrosion-resistant powder materials based on lower and higher nitrides of the Fe-N system in the form of both a bulk composition and a “core-shell” system was implemented at relatively low temperatures. Information on the elemental and chemical composition of iron nitrides was obtained using the methods of Auger electron spectroscopy and X-ray quantitative analysis. Fe3N and Fe4N phases were identified in the volume of microcrystals in the form of compositions with unreacted α-Fe without foreign impurities in the temperature range of 300–350°C. The highest mass concentration of the Fe4N phase was observed at 350°C and a nitriding time of 60 min (α-Fe, 14.70%; Fe3N, 24.50%; and Fe4N, 60.80%). Porous nanocoatings were synthesized on the surfaces of carbonyl iron microparticles at 165°C and a synthesis time of 420 min. This nanocoating has a thickness of ∼10–15 nm and, in the first approximation, corresponds to the ∼Fe15.7N2 compound.
18 schema:genre research_article
19 schema:inLanguage en
20 schema:isAccessibleForFree false
21 schema:isPartOf N41997dd3e840451a9a36210a4b6a3af6
22 N7c9b0231427c47a8b5faa02c796770b9
23 sg:journal.1135943
24 schema:name Low-temperature synthesis of micron nitride powders of the Fe-N system
25 schema:pagination 168-172
26 schema:productId N3b4e9a3345de491cb4c5110f2345e838
27 N86d025aae86a412b853b5489c476be26
28 Nfa9752f27faf49d6be670e3553b60b48
29 schema:sameAs https://app.dimensions.ai/details/publication/pub.1031168821
30 https://doi.org/10.1134/s2075113314020105
31 schema:sdDatePublished 2019-04-10T16:47
32 schema:sdLicense https://scigraph.springernature.com/explorer/license/
33 schema:sdPublisher N2e9212b7c96b4f6781f61c991ccdcff1
34 schema:url http://link.springer.com/10.1134%2FS2075113314020105
35 sgo:license sg:explorer/license/
36 sgo:sdDataset articles
37 rdf:type schema:ScholarlyArticle
38 N2e9212b7c96b4f6781f61c991ccdcff1 schema:name Springer Nature - SN SciGraph project
39 rdf:type schema:Organization
40 N3b4e9a3345de491cb4c5110f2345e838 schema:name doi
41 schema:value 10.1134/s2075113314020105
42 rdf:type schema:PropertyValue
43 N41997dd3e840451a9a36210a4b6a3af6 schema:issueNumber 2
44 rdf:type schema:PublicationIssue
45 N4c06cdad1dad41e9b4793f40965da06c rdf:first sg:person.013524315623.89
46 rdf:rest Nd6fd22df0c9044179c47d8863c22cda2
47 N6d76b400274e489992863d3cc70a73eb rdf:first sg:person.011344617213.59
48 rdf:rest rdf:nil
49 N7c9b0231427c47a8b5faa02c796770b9 schema:volumeNumber 5
50 rdf:type schema:PublicationVolume
51 N86d025aae86a412b853b5489c476be26 schema:name dimensions_id
52 schema:value pub.1031168821
53 rdf:type schema:PropertyValue
54 Nc3b33aefaec749f3a5d8cb84dcd1590c rdf:first sg:person.015657347013.51
55 rdf:rest N4c06cdad1dad41e9b4793f40965da06c
56 Nd06dc04b556a4d1ea3951a57ca89b54f rdf:first sg:person.012234246102.87
57 rdf:rest Nc3b33aefaec749f3a5d8cb84dcd1590c
58 Nd6fd22df0c9044179c47d8863c22cda2 rdf:first sg:person.015550453605.21
59 rdf:rest N6d76b400274e489992863d3cc70a73eb
60 Nfa9752f27faf49d6be670e3553b60b48 schema:name readcube_id
61 schema:value 947c1cbd6d22a259602872f42dac51ddf1fc5076199704672c3cab621e2da4a2
62 rdf:type schema:PropertyValue
63 anzsrc-for:03 schema:inDefinedTermSet anzsrc-for:
64 schema:name Chemical Sciences
65 rdf:type schema:DefinedTerm
66 anzsrc-for:0306 schema:inDefinedTermSet anzsrc-for:
67 schema:name Physical Chemistry (incl. Structural)
68 rdf:type schema:DefinedTerm
69 sg:journal.1135943 schema:issn 2075-1133
70 2075-115X
71 schema:name Inorganic Materials: Applied Research
72 rdf:type schema:Periodical
73 sg:person.011344617213.59 schema:affiliation https://www.grid.ac/institutes/grid.4886.2
74 schema:familyName Zelenskii
75 schema:givenName V. A.
76 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.011344617213.59
77 rdf:type schema:Person
78 sg:person.012234246102.87 schema:affiliation https://www.grid.ac/institutes/grid.4886.2
79 schema:familyName Kovalev
80 schema:givenName E. P.
81 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.012234246102.87
82 rdf:type schema:Person
83 sg:person.013524315623.89 schema:affiliation https://www.grid.ac/institutes/grid.4886.2
84 schema:familyName Ankudinov
85 schema:givenName A. B.
86 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.013524315623.89
87 rdf:type schema:Person
88 sg:person.015550453605.21 schema:affiliation https://www.grid.ac/institutes/grid.4886.2
89 schema:familyName Gnedovets
90 schema:givenName A. G.
91 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.015550453605.21
92 rdf:type schema:Person
93 sg:person.015657347013.51 schema:affiliation https://www.grid.ac/institutes/grid.4886.2
94 schema:familyName Alymov
95 schema:givenName M. I.
96 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.015657347013.51
97 rdf:type schema:Person
98 https://doi.org/10.1002/bbpc.19300360711 schema:sameAs https://app.dimensions.ai/details/publication/pub.1027289743
99 rdf:type schema:CreativeWork
100 https://doi.org/10.1016/j.actamat.2007.08.020 schema:sameAs https://app.dimensions.ai/details/publication/pub.1049627660
101 rdf:type schema:CreativeWork
102 https://doi.org/10.1016/j.jallcom.2005.12.134 schema:sameAs https://app.dimensions.ai/details/publication/pub.1003695195
103 rdf:type schema:CreativeWork
104 https://doi.org/10.1016/j.materresbull.2008.02.008 schema:sameAs https://app.dimensions.ai/details/publication/pub.1001050951
105 rdf:type schema:CreativeWork
106 https://doi.org/10.1016/s0304-8853(99)00429-1 schema:sameAs https://app.dimensions.ai/details/publication/pub.1010306878
107 rdf:type schema:CreativeWork
108 https://doi.org/10.1016/s0304-8853(99)00536-3 schema:sameAs https://app.dimensions.ai/details/publication/pub.1027892221
109 rdf:type schema:CreativeWork
110 https://doi.org/10.1088/0953-8984/6/4/001 schema:sameAs https://app.dimensions.ai/details/publication/pub.1008085971
111 rdf:type schema:CreativeWork
112 https://doi.org/10.1088/1367-2630/12/6/063032 schema:sameAs https://app.dimensions.ai/details/publication/pub.1059135073
113 rdf:type schema:CreativeWork
114 https://doi.org/10.1098/rspa.1951.0155 schema:sameAs https://app.dimensions.ai/details/publication/pub.1043031373
115 rdf:type schema:CreativeWork
116 https://doi.org/10.1103/physrevb.80.024202 schema:sameAs https://app.dimensions.ai/details/publication/pub.1060629627
117 rdf:type schema:CreativeWork
118 https://doi.org/10.2320/matertrans.maw201023 schema:sameAs https://app.dimensions.ai/details/publication/pub.1019102700
119 rdf:type schema:CreativeWork
120 https://www.grid.ac/institutes/grid.4886.2 schema:alternateName Russian Academy of Sciences
121 schema:name Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninskii pr. 49, 119991, Moscow, Russia
122 rdf:type schema:Organization
 




Preview window. Press ESC to close (or click here)


...