Phase Transformations 2,4,6-Tris(2,2,2-Trinitroethylnitramino)-1,3,5-Triazine View Full Text


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Article Info

DATE

2021-07

AUTHORS

V. V. Zakharov, N. V. Chukanov, G. V. Shilov, G. V. Malkov, T. S. Larikova, V. V. Nedelko, A. G. Korepin, B. L. Korsunsky

ABSTRACT

Thermal transformations of 2,4,6-tris(2,2,2-trinitroethylnitramino)-1,3,5-triazine (I) are studied in the temperature range 22–300°C with the use of methods of differential thermal analysis, powder X-ray diffractometry, and IR spectroscopy. At 120°C, the polymorphic transformation α-I → β-I, which is preceded by a sharp increase in the volume of the unit cell and amorphization of I, is recorded. The polymorphic transformation is accompanied by a significant increase in the rate of thermal decomposition of the compound I. Under normal conditions, the phase β-I is stable, but a reverse polymorphic transformation with the formation of a defect phase α-I can be realized at a pressure of 5 kbar. More... »

PAGES

622-629

References to SciGraph publications

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  • 2020-01. Effect of polymorphic phase transitions on stability of energetic compounds. Thermal transformations of 2,4,6-tris(2,2,2-trinitroethylnitramino)-1,3,5-triazine in RUSSIAN CHEMICAL BULLETIN
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  • 2018-01. 2,4,6-Triazido-1,3,5-Triazine, 2,4,6-Triazidopyrimidine, and 2,4,6-Triazidopyridine as Precursors of Carbon Nitride Materials in RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY B
  • 2006-02. Kinetics and mechanism of a polymorphous transition in polycrystalline ε-hexanitrohexaazaisowurtzitane in RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY A
  • 2019-03. Thermal Conversions of 2,4-Bis(N,N-Dimethylamino)-6-Trinitromethyl-1,3,5-Triazine in RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY B
  • 2019-03. Synthesis of 2,4,6-tris(2,2,2-trinitroethylnitramino)-1,3,5-triazine in RUSSIAN CHEMICAL BULLETIN
  • 2014-09. Kinetics of reversible polymorphic transitions in high-energy compounds. Phase transformations in octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine in RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY B
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