Novel Biocomposites Based on El Retma Natural Fiber and PLA/PC Mixture Compatibilized Using Samarium Acetylacetonate Catalyzed Interchange Reactions View Full Text


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Article Info

DATE

2022-04-29

AUTHORS

Ali Larous, Melia Guessoum, Sorya Nekkaa, Magali Fois

ABSTRACT

—In this work, the properties of biocomposites based on poly(lactic acid)/polycarbonate (PLA/PC) mixture and a flour obtained from a local plant which is El Retma (RET) are investigated. Due to the incompatibility of PLA/PC matrix, a transesterification catalyst which is samarium acetylacetonate (Sm) is added to promote interchange reactions and synthesize PLA-PC copolymer at the interface between the polymers. Furthermore, to improve adhesion of the natural fiber to the matrix, RET flour has been pretreated using an alkaline solution before treatment with maleic anhydride (MA). Also, to point out the effect of the rate of MA grafting and RET flour size, the properties of biocomposites based on MA-RET flours with flour sizes below 100 and 50 µm are compared. The composites with mixing time varying from 10 and 20 min have also been studied because they are expected to present different performances due to the different extents of catalyzed transesterification reactions. Fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis attested for the grafting of maleic anhydride grafting after the observation of carbonyl group band in FTIR spectra of MA-RET flour and the improvement of its thermal stability compared to the pretreated flour. The composite PLA/PC/Sm/MA-RET melt mixed during 20 min revealed better impact resistance, thermal stability and storage modulus due to the eventual higher concentration of PLA-PC copolymer and grafting of PLA and PC chains on the flour. More... »

PAGES

1-13

References to SciGraph publications

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  • 2018-03-12. Effect of alkali treatment on wettability and thermal stability of individual bamboo fibers in JOURNAL OF WOOD SCIENCE
  • 2017-02-07. Contribution of Catalytic Transesterification Reactions to the Compatibilization of Poly(lactic acid)/Polycarbonate Blends: Thermal, Morphological and Viscoelastic Characterization in JOURNAL OF POLYMERS AND THE ENVIRONMENT
  • 2018-05-11. Probing the nanomechanical properties of PLA/PC blends compatibilized with compatibilizer and nucleation agent by AFM in JOURNAL OF POLYMER RESEARCH
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  • 2010-10-30. Equilibrium, Kinetics and Mechanism of Removal of Methylene Blue from Aqueous Solution by Adsorption onto Pine Cone Biomass of Pinus radiata in WATER, AIR, & SOIL POLLUTION
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  • 2020-07-24. Packaging Film of PP/LDPE/PLA/Clay Composite: Physical, Barrier and Degradable Properties in JOURNAL OF POLYMERS AND THE ENVIRONMENT
  • 2003-01. Starch, Poly(lactic acid), and Poly(vinyl alcohol) Blends in JOURNAL OF POLYMERS AND THE ENVIRONMENT
  • 2010-12-28. Effect of Nucleating Agents on Physical Properties of Poly(lactic acid) and Its Blend with Natural Rubber in JOURNAL OF POLYMERS AND THE ENVIRONMENT
  • 2014-12. Properties of alkali treated short flax fiber reinforced poly(lactic acid)/polycarbonate composites in FIBERS AND POLYMERS
  • 2012-12-15. Effect of (3-aminopropyl)trimethoxysilane on mechanical properties of PLA/PBAT blend reinforced kenaf fiber in IRANIAN POLYMER JOURNAL
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