Synthesis and Properties of Metathesis Polymer Based on 3-Silatranyltricyclo[4.2.1.02.5]non-7-ene View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-09

AUTHORS

D. A. Alentiev, D. M. Dzhaparidze, P. P. Chapala, M. V. Bermeshev, N. A. Belov, R. Yu. Nikiforov, L. E. Starannikova, Yu. P. Yampolskii, E. Sh. Finkelshtein

ABSTRACT

A new metathesis polynorbornene containing bulky and reactive silatrane side groups is synthesized, and its gas-transport properties are investigated. The metathesis polymerization of 3-silatranyltricyclo[ 4.2.1.02.5]non-7-ene is conducted in the presence of the first-generation Grubbs catalyst. The homopolymer is obtained with a nearly quantitative yield of 98% and a molecular mass of Mw = 1.3 × 106 (Ð = 3.7). According to X-ray phase analysis, the homopolymer is amorphous and its glass-transition temperature is 232°С (DSC). The gas permeability of the metathesis polymer for a set of gases, including He, H2, O2, N2, CO2, and CH4, is investigated, and the corresponding diffusion and solubility coefficients are determined. More... »

PAGES

612-620

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1560090418050019

DOI

http://dx.doi.org/10.1134/s1560090418050019

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1107667925


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