Free-radical cooligomerization of N-vinyl-4,5,6,7-tetrahydroindole with butyl vinyl ether View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-11

AUTHORS

M. V. Markova, I. V. Tatarinova, L. V. Morozova, A. I. Mikhaleva, T. I. Vakul’skaya, S. S. Khutsishvili, G. F. Prozorova, B. A. Trofimov

ABSTRACT

Oligo(N-vinyl-4,5,6,7-tetrahydroindole-co-butyl vinyl ethers) have been synthesized through free-radical cooligomerization with a yield of 84%. The copolymers are readily soluble in organic solvents (benzene, 1,4-dioxane, chloroform, and tetrahydrofuran), stable up to 380–400°C, and paramagnetic. (The concentration of paramagnetic centers is 1014 spin/g.) In addition, the copolymers exhibit the properties of organic semiconductors. (After being doped with iodine, σ = 1.1 × 10−7 S/cm.) The analysis of the 1H and 13C NMR spectra has shown that the oligomerization reaction is complicated by intramolecular cyclization involving carbon atoms located at the 2-position of pyrrole rings. More... »

PAGES

584-592

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1560090413120014

DOI

http://dx.doi.org/10.1134/s1560090413120014

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1032510142


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