Polymers based on ionic monomers with side phosphonate groups View Full Text


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Article Info

DATE

2010-06

AUTHORS

O. A. Mel’nik, A. S. Shaplov, E. I. Lozinskaya, N. A. Popova, M. V. Makarov, I. L. Odinets, K. A. Lysenko, G. I. Timofeeva, I. A. Malyshkina, Ya. S. Vygodskii

ABSTRACT

A number of new ionic vinyl monomers composed of 1-vinylimidazolium cation with diethoxy- and dihydroxyphosphoryl groups and various anions—Br−, (CN)2N−, and (CF3SO2)2N−—are synthesized. The free-radical polymerization of the monomers in solutions of molecular and ionic solvents yields new polymer analogs of ionic liquids, and their molecular-mass characteristics, solubility, heat resistance, thermal stability, and electrical conductivity are estimated. It is shown that the incorporation of bulky phosphorylalkyl side substituents into the vinylimidazolium polycation causes a decrease in the glass-transition temperature and an increase in the ionic conductivity of polymer salts. The highest ionic conductivity (2.6 × 10−5 S/cm at 25°C) is exhibited by the polymer with the (CN)2N− anion. More... »

PAGES

316-326

References to SciGraph publications

  • 2007-03. Synthesis and ionic conductivity of polymer ionic liquids in POLYMER SCIENCE, SERIES A
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