Reactions of 2-(2-propynylsulfanyl)-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-d]pyrimidin-4(3H)-one with arylsulfenyl chlorides View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-10

AUTHORS

A. I. Vas’kevich, R. I. Vas’kevich, V. I. Staninets, S. A. But, A. N. Chernega

ABSTRACT

2-(2-propynylsulfanyl)-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-d]pyrimidin-4(3H)-one with arylsulfenyl chlorides in chloroform gave products of anti-Markownikoff AdE-addition. The use of nitromethane as solvent in the presence of lithium perchlorate additives favored intramolecular electrophilic cyclization into 1-arylsulfanyl-1,2,6,7,8,9-hexahydro-4H-benzo[4,5]thieno[3,2-e][1,3]thiazolo[3,2-a]-pyrimidin-5-one.

PAGES

1526-1531

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s107042800710020x

DOI

http://dx.doi.org/10.1134/s107042800710020x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1041501029


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