Properties of 2-Iodomethyl-2,3-dihydro[1,3]oxazolo[3,2-a]pyridinium Triiodide View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-12

AUTHORS

D. G. Kim, E. V. Kalita, V. V. Sharutin, V. S. Senchurin, V. O. Belov

ABSTRACT

2-Iodomethyl-2,3-dihydro[1,3]oxazolo[3,2-a]pyridinium triiodide was synthesized by the reaction of 1-allylpyridin-2(1H)-one with hydrogen iodide in the presence of hydrogen peroxide or with iodine in acetone. The title compound reacted with palladium(II) iodide in DMSO to give crystalline bis(2-iodomethyl-2,3-dihydro[1,3]oxazolo[3,2-a]pyridinium) di-μ2-iodido-tetraiodidodipalladate(II) whose structure was proved by X-ray analysis. The reaction of 2-iodomethyl-2,3-dihydro[1,3]oxazolo[3,2-a]pyridinium triiodide with sodium iodide in acetone afforded 2-iodomethyl-2,3-dihydro[1,3]oxazolo[3,2-a]pyridinium iodide which decomposed into initial 1-allylpyridin-2(1H)-one and iodine on heating in methanol. More... »

PAGES

2498-2503

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070363218120071

DOI

http://dx.doi.org/10.1134/s1070363218120071

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1113044084


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