Hydrotreating of a Vacuum Gas Oil-Heavy Coker Gas Oil Mixture View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-09

AUTHORS

N. N. Tomina, P. S. Solmanov, N. M. Maksimov, A. V. Moiseev, A. A. Pimerzin, I. I. Zanozina, M. V. Babintseva

ABSTRACT

Changes in the chemical composition of the vacuum gas oil in a mixture with heavy coker gas oil in the presence of industrial and laboratory NiMoW/P2O5–Al2O3 catalyst were studied. The support used was γ-Al2O3, prepared from AlOOH powder TH-60 (Sasol), with the following textural characteristics: SBET = 205 m2/g, Vpore = 0.682 cm3/g, Reff = 48 Å. Alumina was modified with P2O5 by incipient wetness impregnation with a solution of phosphoric acid (reagent grade), followed by drying and calcination. The catalysts were prepared by incipient wetness impregnation with a combined solution of Mo, W, and Ni compounds. Before the catalytic test, the catalysts were subjected to sulfidation directly in the hydrotreating reactor of a laboratory setup in a stream of H2S/H2 = 70/30 vol %/vol % under 0.11 MPa pressure for 2 h at 500°C. The catalytic properties of the catalysts synthesized were examined under the following conditions: temperature of 360 and 390°C, hydrogen pressure of 5.0 MPa, liquid hourly space velocity of 1.0 h–1, volume ratio of hydrogen to feed of 1000: 1 nL/L, catalyst loading (0.50–0.25 mm fraction) 27 cm3. The reactor temperature was controlled accurately to within 1°C, pressure, to within 0.1 MPa, feed rate, to within 0.2 mL/h, and hydrogen flow, to within 0.2 L/h. During the process the contents of sulfur and polycyclic aromatic hydrocarbons, as well as the hydrocarbon-type content and carbon content of the feed and the hydrogenates, were determined. After the tests the catalysts were studied by differential thermal analysis in combination with thermogravimetry (DTA-TGA). More... »

PAGES

1963-1969

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Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070363218090372

DOI

http://dx.doi.org/10.1134/s1070363218090372

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1109910069


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