Disulfide derivatives of thiosemicarbazones of 4-formyl-5-thiopyrazole View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-02

AUTHORS

A. I. Uraev, M. S. Korobov, L. D. Popov, G. G. Aleksandrov, E. V. Korshunova, D. A. Garnovskii, A. S. Burlov

ABSTRACT

The reaction of 4-formyl-5-mercaptopyrazole with thiosemicarbazides in methanol has afforded novel disulfide derivatives of thiosemicarbazones, and their structure has been studied by NMR and IR spectroscopy. X-ray diffraction analysis of [5,5'-dithiobis(4-formyl-3-methyl-1-phenylpyrazole)]-4-allylthio-semicarbazone has shown that it exists as a dimer with two molecules linked via the disulfide S–S bridge between the heterocycles in the crystal. More... »

PAGES

252-258

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070363217020165

DOI

http://dx.doi.org/10.1134/s1070363217020165

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1084608526


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