Atom-sparing synthesis of tertiary diphosphine dichalcogenides from acetylenes and secondary phosphine chalcogenides View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-02

AUTHORS

S. F. Malysheva, N. A. Belogorlova, V. A. Kuimov, N. I. Ivanova, P. A. Volkov, I. A. Ushakov, N. K. Gusarova, B. A. Trofimov

ABSTRACT

Secondary phosphine oxides and phosphine sulfides react with acetylene, methylacetylene, and phenylacetylene in the presence of strong bases (KOH-DMSO, KOH-THF) by the mechanism of double nucleophilic α,β-addition to form tertiary diphosphine dioxides and diphosphine disulfides in high yield (up to 97%).

PAGES

232-238

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070363210020076

DOI

http://dx.doi.org/10.1134/s1070363210020076

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1002353873


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