Generation of Long-Lived Phenoxyl Radical in the Binuclear Copper(II) Pivalate Complex with 2,6-Di-tert-butyl-4-(3,5-bis(4-pyridyl)pyridyl)phenol View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2022-07-05

AUTHORS

V. N. Dorofeeva, A. V. Pavlishchuk, M. A. Kiskin, N. N. Efimov, V. V. Minin, K. S. Gavrilenko, S. V. Kolotilov, V. V. Pavlishchuk, I. L. Eremenko

ABSTRACT

A new binuclear copper(II) complex Cu2(Piv)4(L)2, where Piv– = pivalate, L = 2,6-di-tert-butyl-4-(3,5-bis(4-pyridyl)pyridyl)phenol, was synthesized, and its molecular and crysral structures were determined at temperatures of 160, 173, and 296 K (CIF files CCDC no. 2144104, 2144105, and 2144106, respectively). Cyclic voltammetry measurements revealed three irreversible oxidation processes in the potential range of 0.5–1.2 V versus Fc+/Fc. Analysis of the temperature dependence of the magnetic susceptibility of Cu2(Piv)4(L)2 showed that antiferromagnetic interactions of Cu2+ ions predominate in the complex. It was found that the oxidation of Cu2(Piv)4(L)2 upon grinding with PbO2 or treatment of a solid sample with an aqueous solution of K3[Fe(CN)6] affords long-lived phenoxyl radical, which can be detected by ESR spectroscopy. More... »

PAGES

422-429

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328422070041

DOI

http://dx.doi.org/10.1134/s1070328422070041

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1149242285


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