Tetra- and Pentanuclear Iodobismuthates with the Cation Based on 2,3,5,6-Tetramethylpyrazine: Syntheses and Crystal Structures View Full Text


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Article Info

DATE

2018-12

AUTHORS

A. N. Usoltsev, S. A. Adonin, P. A. Abramov, M. N. Sokolov, V. P. Fedin

ABSTRACT

Complexes (HTMP)4[Bi4I16] · 2H2O · 2(CH3)2CO (I) and (HTMP)3[Bi5I18] · 5THF (II) have been synthesized by the reactions of BiI3 and 2,3,5,6-tetramethylpyrazine (TMP) in acetone and tetrahydrofuran (THF), respectively. The crystal structures of both compounds were determined by X-ray diffraction analysis (СIF files CCDC nos. 1817306 (I) and 1817307 (II)). In both cases, the complexes in the solid state feature supramolecular contacts between the π systems of the cations and iodide ligands of the anions. More... »

PAGES

772-778

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328418120102

DOI

http://dx.doi.org/10.1134/s1070328418120102

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44 schema:description Complexes (HTMP)4[Bi4I16] · 2H2O · 2(CH3)2CO (I) and (HTMP)3[Bi5I18] · 5THF (II) have been synthesized by the reactions of BiI3 and 2,3,5,6-tetramethylpyrazine (TMP) in acetone and tetrahydrofuran (THF), respectively. The crystal structures of both compounds were determined by X-ray diffraction analysis (СIF files CCDC nos. 1817306 (I) and 1817307 (II)). In both cases, the complexes in the solid state feature supramolecular contacts between the π systems of the cations and iodide ligands of the anions.
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