Synthesis and physicochemical studies of the compounds based on [Ni(Dien)(NH3)3]2+ and [Ni(Trien)(NH3)2]2+ cations and [Re6Se8(CN)4(OH)2]4– octahedral cluster anion View Full Text


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Article Info

DATE

2016-11

AUTHORS

A. V. Ermolaev, A. I. Smolentsev, Yu. V. Mironov

ABSTRACT

Two new compounds, [Ni(Dien)(NH3)3]2[Re6Se8(CN)4(OH)2] • 5.5H2O (I) and [Ni(Trien)(NH3)2]2[Re6Se8(CN)4(OH)2] • 4.67H2O (II) (Dien is diethylenetriamine and Trien is triethylenetetraamine), are synthesized by layering solutions of NiCl2 • 6H2O in aqueous ammonia with the addition of the corresponding amines onto an aqueous solution of cluster salt Cs2.75K1.25[Re6Se8(CN)4(OH)2] • H2O. The structures of both complexes are determined by single-crystal X-ray diffraction analysis (CIF files CCDC 1446999 (I) and 1447000 (II)). The compounds are characterized by IR spectroscopy and elemental and thermogravimetric analyses. More... »

PAGES

730-736

References to SciGraph publications

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