Synthesis and structure of polycrystalline adducts of Co(II) azomethine complexes with redox-active 2,4,6,8-tetrakis-(tert-butyl)phenoxazin-1-one View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-04

AUTHORS

E. P. Ivakhnenko, Yu. V. Koshchienko, P. A. Knyazev, V. B. Nalbandyan, K. A. Lyssenko, I. V. Ananyev, A. S. Bogomyakov, V. I. Minkin

ABSTRACT

The six-coordinate cobalt complexes, C57H63.50N4.50O4Co (IIa), C60H69N5O4Co (IIb), C58H67N3O8Co (IIc), C56H61N5O10Co (IId), C56H63N3O6Co (IIe), C58H66N4O6Co (IIf), and C58H63N7O8Co (IIg), adducts of high-spin tetrahedral Co(II) bis(salicylaldiminates) (C29H24.50N3.50O2Co (Ia), C32H30N4O2Co (Ib), C30H28N2O6Co (Ic), C28H22N4O8Co (Id), C28H24N2O4Co (Ie), C30H27N3O4Co (If), and C30H24N6O6Co (Ig)) and redox-active 2,4,6,8-tetrakis(tert-butyl)phenoxazin-1-one (L), were synthesized and studied for structure and magnetic properties. Complexes IIa–IIg have octahedral structure (CIF files CCDC nos. 1403920 (IIf), 1403922 (IIg)) and exist in the ground low-spin state (ls-CoIII-SQ), which arises upon intramolecular single-electron redox process in the ligand–metal system. The presence of substituents of different nature in the azomethine ligands of IIa–IIg does not induce any significant changes in their magnetic properties. More... »

PAGES

252-259

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328416040011

DOI

http://dx.doi.org/10.1134/s1070328416040011

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