A double complex Cd(II) salt containing the Keggin polyoxoanion and the supramolecular cation of the [amide…H…amide]+ type View Full Text


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Article Info

DATE

2015-10

AUTHORS

S. A. Adonin, L. I. Udalova, A. I. Smolentsev, M. N. Sokolov, V. P. Fedin

ABSTRACT

The complex [H(DMFA)2]2[Cd(DMFA)6][SiW12O40] (I) was obtained by a reaction between H4[SiW12O40], CdI2, and AgNO3 in N,N-dimethylformamide (DMF) and characterized by X-ray diffraction (CIF file CCDC No. 1041227). Structure I is made up of the complex cations [Cd(DMF)6]2+, the Keggin polyoxoanions [SiW12O40]4–, and the dimeric cations [DMF...H...DMF]+, in which two DMF molecules are linked by a short hydrogen bond (O...O, 2.39(2) Å). The cations of this type were compared with similar dimeric cations containing the fragment {amide...H...amide}. More... »

PAGES

633-637

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Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328415100012

DOI

http://dx.doi.org/10.1134/s1070328415100012

DIMENSIONS

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46 schema:description The complex [H(DMFA)2]2[Cd(DMFA)6][SiW12O40] (I) was obtained by a reaction between H4[SiW12O40], CdI2, and AgNO3 in N,N-dimethylformamide (DMF) and characterized by X-ray diffraction (CIF file CCDC No. 1041227). Structure I is made up of the complex cations [Cd(DMF)6]2+, the Keggin polyoxoanions [SiW12O40]4–, and the dimeric cations [DMF...H...DMF]+, in which two DMF molecules are linked by a short hydrogen bond (O...O, 2.39(2) Å). The cations of this type were compared with similar dimeric cations containing the fragment {amide...H...amide}.
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