Influence of morphology and defects in crystals of porous coordination polymers on the sorption characteristics View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-06

AUTHORS

R. A. Polunin, V. N. Dorofeeva, A. E. Baranchikov, V. K. Ivanov, K. S. Gavrilenko, M. A. Kiskin, I. L. Eremenko, V. M. Novotortsev, S. V. Kolotilov

ABSTRACT

Porous coordination polymers [Fe2MO(Piv)6(L)x]n (L is tris(4-pyridyl)pyridine, M = Ni (I) and Co (II); L is tris(4-pyridyl)triazine, M = Ni (III) and Co (IV); x varies from 0.7 to 1.17) are obtained. The structure of polymer I is determined by X-ray diffraction analysis. The choice of the solvent (chloroform or dimethylformamide (DMF)) for the preparation of polycrystalline samples affects the morphology of the crystals. It is found for the studied samples that an increase in the average crystal size (from 1 to 20 μm) and the enhancement of the crystallinity of the samples increase the sorption capacity with respect to hydrogen from 0.7 to 0.9% (78 K, 1 atm). More... »

PAGES

353-361

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328415060056

DOI

http://dx.doi.org/10.1134/s1070328415060056

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1021024149


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