Spin crossover in heteroligand iron(II) complexes with iris(3,5-dimethylpyrazol-1-yl)methane View Full Text


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Article Info

DATE

2015-03

AUTHORS

L. G. Lavrenova, A. D. Strekalova, A. S. Bogomyakov, E. V. Korotaev, A. V. Virovets, D. A. Piryazev, L. A. Sheludyakova, S. F. Vasilevskii

ABSTRACT

Heteroligand iron(II) complexes with tris(3,5-dimethylpyrazol-1-yl)methane (HC(3,5-Me2Pz)3) are synthesized. Along with this ligand, the internal coordination sphere of Fe(II) of the new complexes includes other nitrogen-containing heterocycles, in particular, tetrazole (Tz), pyrazole (Pz), 3,5-dimethylpyrazole (3,5-Me2Pz), and 3-amino-4-ethoxycarbonylpyrazole (Ametcpz), as well as ions NCS− or N(CN)2−. Compounds [Fe(HC(3,5-Me2Pz)3)(Tz)3](NO3)2 (I), [Fe(HC(3,5-Me2Pz)3)(Tz)3](ClO4)2 (II), [Fe(HC(3,5-Me2Pz)3)(Pz)3](NO3)2 (III), [Fe(HC(3,5-Me2Pz)3)(Aecpz)(NCS)2] (IV), and [Fe(HC(3,5-Me2Pz)3)(3,5-Me2Pz)(N(CN)2)2] · 0.5H2O (V) are isolated. The study of the temperature dependence μeff(T) shows the spin crossover 1A1 ⇔ 5T2 accompanied by thermochromism (the color changes from white to pink) in complexes I, II, and IV. The molecular and crystal structures of complex V are determined by X-ray diffraction analysis (CIF file CCDC 994626). More... »

PAGES

189-196

References to SciGraph publications

  • 2012-08. Spin crossover in the coordination compounds of iron(II) with tris(3,5-dimethylpyrazol-1-yl)methane in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
  • 2004. Spin Crossover—An Overall Perspective in SPIN CROSSOVER IN TRANSITION METAL COMPOUNDS I
  • 2008-04. Spin transition in iron(III) and iron(II) complexes in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
  • 2004. Spin Crossover in Pyrazolylborate and Pyrazolylmethane Complexes in SPIN CROSSOVER IN TRANSITION METAL COMPOUNDS I
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    http://scigraph.springernature.com/pub.10.1134/s1070328415030082

    DOI

    http://dx.doi.org/10.1134/s1070328415030082

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