Syntheses, structures, magnetic properties, and photoluminescence of compounds Ln(2,2′-Bipy)(C4H8NCS2)3 · 0.5CH2Cl2 (Ln = Sm, Eu, Tb, Dy, and Tm) View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-10

AUTHORS

Yu. A. Bryleva, L. A. Glinskaya, I. V. Korol’kov, A. S. Bogomyakov, M. I. Rakhmanova, D. Yu. Naumov, T. E. Kokina, S. V. Larionov

ABSTRACT

Five compounds of the composition Ln(2,2′-Bipy)(C4H8NCS2)3 · 0.5CH2Cl2 (Ln = Sm (I), Eu (II), Tb (III), Dy (IV), and Tm (V); 2,2′-Bipy = 2,2′-bipyridine) are synthesized. According to the X-ray diffraction data (CIF file CCDC 986259), the crystal structure of compound I consists of molecules of the mononuclear complex [Sm(2,2′-Bipy)(C4H8NCS2)3] and solvate molecules CH2Cl2 (2 : 1). The coordination polyhedron N2S6 of the Sm atom is a distorted tetragonal antiprism. The X-ray diffraction analysis shows that compounds I–V are isostructural. The magnetic properties of compounds I–V are analyzed in the temperature range from 2 to 300 K. At 300 K compounds I and III are photoluminescent in the visible spectral range. The photoluminescence intensity of compound I considerably exceeds that of complex III. More... »

PAGES

740-747

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328414100029

DOI

http://dx.doi.org/10.1134/s1070328414100029

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1025668210


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