Stannylene complexes of manganese, iron, and platinum View Full Text


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Article Info

DATE

2014-03

AUTHORS

S. S. Shapovalov, A. A. Pasynskii, Yu. V. Torubaev, I. V. Skabitskii, M. Scheer, M. Bodensteiner

ABSTRACT

A number of stannylene complexes with different M: Sn ratios were obtained using various metals and substituents at the tin atom. The structures of the complexes were examined. A reaction of CpMn(CO)2THF with (Ph4As)+(SnCl3)− gave the ionic complex [Ph4As]+[CpMn(CO)2SnCl3]− (I). The action of C6F5MgBr on the complex C5H5Mn(CO)(NO)SnCl3 produced C5H5Mn(CO)(NO)Sn(C6F5)3 (II). Replacement of the Cl ions in the complex [CpFe(CO)2]2SnCl2 by phenylacetylenide groups gave rise to the neutral complex [CpFe(CO)2]2Sn(C≡CPh)2 (III). A reaction of (Dppm)PtCl2 (Dppm is 1,1-bis(diphenylphosphino)methane) with SnCl2 · 2H2O in the presence of diglyme yielded the ionic complex [η3-CH3O(CH2)2O(CH2)2OCH3)SnCl]+[(η 2-Dppm)Pt(SnCl3)3]− (IV). Transmetalation in a reaction of [(Dppe)2CoCl][SnCl3] · PhBr (Dppe is 1,2-bis(diphenylphosphino)ethane) with (Dcpd)PtCl2 (Dcpd is dicyclopentadiene) in the presence of SnCl2 afforded the ionic complex [Pt(Dppe)2]3[Pt(SnCl3)5]2 (V). Structures I–V were identified by X-ray diffraction. In these structures, the formally single bonds between the atoms of transition metals M (Mn, Fe, and Pt) and Main Group heavy elements (Sn and P) having vacant d orbitals are appreciably shortened. The M-Sn bond length in complexes II and III are virtually independent of the substituents at the tin atom and the Pt-Sn bond length in complexes IV and V is virtually independent of the Pt: Sn ratio. More... »

PAGES

131-137

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328414030087

DOI

http://dx.doi.org/10.1134/s1070328414030087

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https://app.dimensions.ai/details/publication/pub.1017002156


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