Mixed-ligand cluster [Mo3S4(Dtp)2(μ-AcO)Cl(Me2Bipy)]: Synthesis and structure View Full Text


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Article Info

DATE

2014-01

AUTHORS

A. L. Gushchin, Yu. A. Laricheva, D. A. Piryazev, M. N. Sokolov

ABSTRACT

Mixed-ligand cluster [Mo3S4(Dtp)2(μ-AcO)Cl(Me2Bipy)] · CHCl3 (I · CHCl3), where Dtp is (EtO)2PS2, was synthesized by the reaction of the molybdenum aqua complex [Mo3S4(H2O)9]4+ with 4,4′-dimethyl-2,2′-bipyridine (Me2Bipy) and phosphorus sulfide (P4S10) in ethanol followed by chromatographic separation on silica gel and crystallization in the presence of acetic acid. The crystal structure of I · CHCl3 was determined by X-ray diffraction analysis. The synthesized compound was characterized by the IR and NMR spectra and elemental analysis. The electronic structure of the synthesized compound was established, and its electrochemical behavior in a solution was studied. More... »

PAGES

5-9

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328414010023

DOI

http://dx.doi.org/10.1134/s1070328414010023

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