Direct electrochemical and chemical syntheses, structures, and properties of metal complexes of azo compounds with an additional azo group in ... View Full Text


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Article Info

DATE

2013-12

AUTHORS

A. S. Burlov, S. A. Mashchenko, A. S. Antsyshkina, G. G. Sadikov, V. S. Sergienko, M. A. Kiskin, S. A. Nikolaevskii, V. G. Vlasenko, Ya. V. Zubavichus, A. I. Uraev, D. A. Garnovskii, E. V. Korshunova, S. I. Levchenkov

ABSTRACT

New complexes of Cu(II), Co(II), and Ni(II) with 1-phenyl-3-methyl-4-[(4-phenylazophenyl)hydrazono]-5H-pyrazol-5-one and 1-phenyl-3-methyl-4-[4-methyl-2-(4-methylphenylazophenyl)hydrazono]-5H-pyrazol-5-one are synthesized by the chemical and electrochemical methods and characterized by IR, 1H NMR, and EXAFS spectroscopy and X-ray diffraction analysis. Depending on the complexing metal and position of the additional azo group, the latter is involved or not in coordination with the metal to form heterounit five- and six-membered metallocycles. More... »

PAGES

813-821

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328413120014

DOI

http://dx.doi.org/10.1134/s1070328413120014

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1021297357


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