Synthesis, X-ray spectral, and magnetochemical study of copper complexes based on tridentate azomethines of 3-allylsalicylaldehyde View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-04

AUTHORS

A. S. Burlov, V. G. Vlasenko, Ya. V. Zubavichus, S. I. Levchenkov, Yu. V. Koshchienko, A. S. Bogomyakov, S. A. Nikolaevskii, D. A. Garnovskii, A. I. Uraev, T. V. Lifintseva, E. V. Korshunova

ABSTRACT

Tridentate azomethine ligands (H2L) based on 3-allylsalicylaldehyde and o-aminophenol, o-aminothiophenol, or 2-ethylamino-5-nitroaniline were synthesized and identified by IR and 1H NMR spectroscopies. The structure of complexes (Ia-Ic) was studied by magnetochemistry and EXAFS spectroscopy. Complexes Ia and Ib (X = O, S) are binuclear and exhibit antiferromagnetic exchange interaction: 2J = −36.5 and −950 cm−1, respectively. Complex Ic (X = NC2H5) is mononuclear (μeff = 1.75 μB at 275 K and does not change as temperature decreases). More... »

PAGES

347-352

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URI

http://scigraph.springernature.com/pub.10.1134/s1070328413040039

DOI

http://dx.doi.org/10.1134/s1070328413040039

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