Spin crossover in the coordination compounds of iron(II) with tris(3,5-dimethylpyrazol-1-yl)methane View Full Text


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Article Info

DATE

2012-08

AUTHORS

L. G. Lavrenova, A. D. Strekalova, A. V. Virovets, D. A. Piryazev, V. A. Daletskii, L. A. Sheludyakova, T. F. Mikhailovskaya, S. F. Vasilevskii

ABSTRACT

Iron(II) complexes with tris(3,5-dimethylpyrazol-1-yl)methane {HC(3,5-Me2Pz)3} of the composition [Fe{HC(3,5-Me2Pz)3}2]Am · nH2O (A = Cl− (I), ClO4−(II), SO42−(III), CF3SO3−(IV), m = 1, 2, n = 0.1) are synthesized. The compounds are studied by static magnetic susceptibility, IR and diffuse reflectance spectroscopy, and X-ray structure analysis. The crystal structures of two polymorphous modifications of the [Fe{HC(3,5-Me2Pz)3}2](ClO4)2 (IIa and IIb) and [Fe{HC(3,5-Me2Pz)3}2](CF3SO3)2 (IV) complexes are determined. The temperature dependence μeff(T) shows that the spin crossover 1A1 ai 5T2 is observed in the polycrystalline phase of complex I and in one of the single-crystal phases of complex II (IIa) and is accompanied by thermochromism (the change of the dark pink color ai to white). More... »

PAGES

507-514

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328412070081

DOI

http://dx.doi.org/10.1134/s1070328412070081

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