New nickel(II) carboxylate-phosphonate cluster: Synthesis and structure View Full Text


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Article Info

DATE

2012-05

AUTHORS

N. P. Burkovskaya, M. E. Nikiforova, M. A. Kiskin, V. I. Pekhn’o, A. A. Sidorov, V. M. Novotortsev, I. L. Eremenko

ABSTRACT

Dodecanuclear mixed-ligand complex [(μ2-Hmhp)6Ni12(μ3-OH)4(μ6-O3PPh)4(μ2-Piv)12] · 7.5MeCN · 1.5THF (I · 7.5MeCN · 1.5THF) was synthesized by the reaction of nickel(II) trimethylacetate [Ni9(OH)6(Piv)12(HPiv)4] (Piv− is the pivalate anion) and 6-methyl-2-hydroxypyridine (Hmhp) with phenylphosphonic acid potassium salt (K2O3PPh). The structure of complex I is determined by X-ray diffraction analysis. The geometry of the metal framework of the isolated complex is determined by the structure forming phosphonate anion. More... »

PAGES

331-336

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328412050016

DOI

http://dx.doi.org/10.1134/s1070328412050016

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1051028421


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