Heterometallic clusters with the {MoNbI8} core: The synthesis and crystal structures of (Ph4P)2[Mo5NbI8Cl6] and (4-MePyH)5[Mo5NbI8Cl6]Cl2 View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-04

AUTHORS

S. B. Artemkina, M. S. Tarasenko, A. V. Virovets, N. G. Naumov

ABSTRACT

Heterometallic chloride complexes [Mo5NbI8Cl6]n− (n = 2, 3) are synthesized. The crystal structures of their salts are determined: for (Ph4P)2[Mo5NbI8Cl6] (I), triclinic crystal system, spacegroup P, a = 10.9886(6), b = 11.4604(5), c = 13.4343(7) Å, α = 66.124(2), β = 86.892(2), γ = 86.490(2)°, Z = 1, V = 1543.35(13) Å3; and for (4-MePyH)5[Mo5NbI8Cl6]Cl2 (II), monoclinic crystal system, space group C2/m, a = 16.4937(4), b = 14.7335(3), c = 11.6534(3) Å, β = 99.8750(10)°, Z = 2, V = 2789.94(11) Å The geometric parameters of compounds I and II and the conditions for the formation of the complexes with the charges −2 and −3 are discussed. More... »

PAGES

257-263

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328412030013

DOI

http://dx.doi.org/10.1134/s1070328412030013

DIMENSIONS

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