Different ways of coordination for aminoalkyldiphosphonic acids in palladium(II) complexes View Full Text


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Article Info

DATE

2011-12

AUTHORS

A. N. Kozachkova, A. V. Dudko, N. V. Tsaryk, V. V. Trachevskii, A. B. Rozhenko, V. I. Pekhnyo

ABSTRACT

Complexation in the systems K2PdCl4-3-amino-1-hydroxypropane-1,1-diyldiphosphonic acid (AHPDP) and K2PdCl4-1-aminoethane-1,1-diyldiphosphonic acid (AEDP) was studied using pH-potentiometry, spectrophotometry, and 31P NMR spectroscopy. It was found that AHPDP in equimolar complexes is coordinated by Pd(II) in a bidentate fashion through two phosphonate O atoms forming a six-membered chelate [O,O]-ring, while AEDP is coordinated through the N atom and one phosphonate O atom forming a five-membered chelate [N,O]-ring. In 1: 2 complexes of Pd(II) with AEDP, the second AEDP molecule is coordinated by Pd(II) in a similar way to form a second five-membered [N,O]-ring. The latter complexes show cis-trans and syn-anti isomerism. The structural characteristics of the corresponding isomers were calculated at the DFT level of theory and their stabilities were compared. More... »

PAGES

941-948

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328411120025

DOI

http://dx.doi.org/10.1134/s1070328411120025

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1045448618


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