Complexes of copper(II) and cobalt(II) halides with 4-(3,5-dimethyl-1H-pyrazol-1-yl)-6-methyl-2-phenylpyrimidine: Synthesis, structures, and properties View Full Text


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Article Info

DATE

2009-08

AUTHORS

M. B. Bushuev, V. P. Krivopalov, E. V. Peresypkina, A. V. Virovets, Yu. G. Shvedenkov, L. A. Sheludyakova, N. V. Semikolenova, V. A. Zakharov, S. V. Larionov

ABSTRACT

Copper(II) and cobalt(II) complexes with 4-(3,5-dimethyl-1H-pyrazol-1-yl)-6-methyl-2-phenylpyrimidine (L) of the general formula MLX2 (M = Cu(II), X = Cl and Br; M = Co(II), X = Cl, Br, and I) were obtained. According to X-ray diffraction data, CuLBr2 and CoLX2 (X = Cl, Br, and I) are mononuclear molecular complexes. The ligand L is coordinated to the metal atom in a chelating bidentate fashion through the N atoms of the pyrimidine and pyrazole rings. The coordination polyhedron of the metal atom is extended to a distorted tetrahedron by two halide ions. In solution, CuLBr2 undergoes slow transformation into CuL(1−x)L′xBr2 and the binuclear (X-ray diffraction data) Cu(I) complex [CuL(1−x)L′xBr]2 (L′ is 4-(4-bromo-3,5-dimethyl-1H-pyrazol-1-yl)-6-methyl-2-phenylpyrimidine). The complexes MLX2 show weak antiferromagnetic interactions between the M2+ ions. More... »

PAGES

597-608

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328409080077

DOI

http://dx.doi.org/10.1134/s1070328409080077

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