Copper(II) and cobalt(II) complexes with a chiral 5-pyrazolone derivative obtained from the terpene (+)-3-carene: Synthesis and properties View Full Text


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Article Info

DATE

2008-10

AUTHORS

Z. A. Savel’eva, L. A. Glinskaya, R. F. Klevtsova, E. G. Boguslavskii, S. A. Popov, N. V. Semikolenova, A. V. Tkachev, V. A. Zakharov, S. V. Larionov

ABSTRACT

The complexes [CuLCl2] (I), [CoLCl2] (II), and CuLBr2 (III) (where L is the derivative of optically active 5-pyrazolone prepared from the terpene (+)-3-carene) were obtained and characterized. According to X-ray diffraction data, crystal structures I and II (orthorhombic crystal system) are built from mononuclear acentric molecules. In the resulting complexes, the Cu2+ or Co2+ ion coordinates two N atoms of the chelating bidentate ligand L and two Cl atoms, thus making a distorted tetrahedron. Intermolecular contacts and the hydrogen bonds Cl(1)…H-O(1) give rise to columns parallel to axis y. For complexes I and III, μeff = 1.83 and 1.81 μB, respectively; these values correspond to the electronic configuration d9. For complex II, μeff = 4.42 μB, which suggests the tetrahedral structure of the coordination entity CoCl2N2. Complexes I and III were studied by EPR spectroscopy. More... »

PAGES

766-771

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328408100102

DOI

http://dx.doi.org/10.1134/s1070328408100102

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1016837415


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