Cu(II) and Cu(I) complexes with 2-(3,5-diphenyl-1H-pyrazole-1-yl)-4,6-diphenylpyrimidine: Synthesis and structure. Catalytic activity of Cu(II) compounds in reaction of ethylene polymerization View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2006-03

AUTHORS

M. B. Bushuev, V. P. Krivopalov, N. V. Semikolenova, E. V. Peresypkina, A. V. Virovets, L. A. Sheludyakova, L. G. Lavrenova, V. A. Zakharov, S. V. Larionov

ABSTRACT

The Cu(II) and Cu(I) complexes with 2-(3,5-diphenyl-1H-pyrazole-1-yl)-4,6-diphenylpyrimidine (L) of the composition CuLX2 (X = Cl, Br) and CuL(MeCN)Br are synthesized. According to X-ray diffraction data, the complexes have molecular structures. The molecules L are coordinated to the copper atom in bidentate-cyclic mode, i.e., through the N2 atom of pyrazole and N1 atom of pyrimidine rings. The coordination polyhedron of the Cu2+ ion in CuLX2 compounds is completed to a distorted tetrahedron with halide ions, that of the Cu+ ion in CuL(MeCN)Br compounds, with the bromide ion and the nitrogen atom of acetonitrile molecule. The CuLX2 complexes (X = Cl, Br) in combination with cocatalysts (methylaluminoxane and triisobutylaluminium) exhibit catalytic activity in ethylene polymerization. More... »

PAGES

199-207

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1070328406030067

DOI

http://dx.doi.org/10.1134/s1070328406030067

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1017106009


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