Interaction of sodium fullerene derivatives with trimethylchlorosilane View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2006-05

AUTHORS

S. N. Titova, G. A. Domrachev, E. A. Gorina, L. V. Kalakutskaya, A. M. Ob”edkov, B. S. Kaverin, S. Yu. Ketkov, M. A. Lopatin, A. V. Markin, N. N. Smirnova, K. B. Zhogova

ABSTRACT

Soluble dimer compounds of the general formula [C60(Me3Si)n]2 (where n = 3, 5, 7, or 9 and Me = CH3) and a soluble monomer compound, C60(Me3Si)12, are synthesized by the reaction of the compound C60Nan(THF)x (where n = 4, 6, 8, 10, or 12 and THF = tetrahydrofuran) with trimethylchlorosilane Me3SiCl. The compounds synthesized are identified using IR and NMR spectroscopy and mass spectrometry. An irreversible endothermic effect exhibited by the [C60(Me3Si)7]2 compound in the temperature range 448–570 K is revealed by dynamic adiabatic calorimetry. From analyzing the experimental results, it becomes possible for the first time to demonstrate the structural flexibility of the fullerene in the following sequence of reactions: More... »

PAGES

1000-1006

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1063783406050301

DOI

http://dx.doi.org/10.1134/s1063783406050301

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1015229718


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