Orthorhombic YBaCo4O8.4 crystals as a result of saturation of hexagonal YBaCo4O7 crystals with oxygen View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-07

AUTHORS

N. V. Podberezskaya, N. B. Bolotina, V. Yu. Komarov, M. Yu. Kameneva, L. P. Kozeeva, A. N. Lavrov, A. I. Smolentsev

ABSTRACT

Hexagonal YBaCo4O7 crystals (sp. gr. P63mc, ah = 6.3058(4) Å, ch = 10.2442(7) Å, Z = 2) are saturated with oxygen to the YBaCo4O8.4 composition and studied by X-ray diffraction (XRD) analysis. The saturation is completed by a structural first-order phase transition to orthorhombic crystals (sp. gr. Pbc21, ao = 31.8419(2) Å, bo = 10.9239(5) Å, co = 10.0960(5) Å, Z = 20). The connection of two lattices is expressed in terms of the action of matrix (500/120/001) on the hexagonal basis. Five structural fragments of the same type but with different degrees of order alternate along the long axis of the oxygen-saturated orthorhombic structure. The XRD data on single crystals differ from the results obtained by other researchers on ceramic samples; possible causes of these differences are discussed. More... »

PAGES

484-492

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1063774515040161

DOI

http://dx.doi.org/10.1134/s1063774515040161

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1012323357


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