Crystal structures of bis(cyanido)bis(N,N′-diethylthiourea-κS) mercury(II) and bis(cyanido)bis(N,N′-dipropylthiourea-κS) mercury(II) View Full Text


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Article Info

DATE

2013-09

AUTHORS

Saeed Ahmad, Haseeba Sadaf, Muhammad Altaf, Helen Stoeckli-Evans, Seerat-ur-Rehman, Sarfaraz Ahmed Bashir

ABSTRACT

Two mercury(II) complexes containing cyanide and, N,N′-diethylthiourea (detu) and N,N′-dipropylthiourea (dprtu) ligands, [(detu)2Hg(CN)2] (1) and [(dprtu)2Hg(CN)2] (2), respectively, have been prepared and characterized by X-ray crystallography. In the both complexes Hg atom lies on a 2-fold rotation axis, and is coordinated to the sulfur atoms of two thiourea ligands and to two cyanide carbon atoms. Both have a distorted tetrahedral environment with bond angles about the Hg atoms in the range of 93.41(4)°–146.75(19)°. In the crystal structures symmetry related molecules are linked via N-H-N hydrogen bonds resulting in the formation of a two-dimensional network in 1, while in 2 a double stranded one-dimensional chain is formed. More... »

PAGES

692-696

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s1063774513050155

DOI

http://dx.doi.org/10.1134/s1063774513050155

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1007067582


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