Effect of IR Radiation on the Properties of Polyacrylonitrile and Membranes on Its Basis View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-11

AUTHORS

A. A. Yushkin, M. N. Efimov, A. A. Vasil’ev, V. I. Ivanov, Yu. G. Bogdanova, V. D. Dolzhikova, G. P. Karpacheva, G. N. Bondarenko, A. V. Volkov

ABSTRACT

The effect of processing of polyacrylonitrile membranes by IR radiation at a temperature of 100–150°С is studied. The influence of the processing temperature on the film structure is ascertained. In a film heated at 100°С, a small amount of the double C=N bonds is found. Its further heating to 120°С is accompanied by a change in the chain conformation and an increase in the content of C=N bonds. It is shown that, upon IR processing at 120°С, polyacrylonitrile ceases to dissolve in N-methylpyrrolidone, dimethylacetamide, dimethylformamide, and dimethyl sulfoxide. Heating at 150°С gives rise to the appearance of conjugated С=N–C=N bonds. The analysis of AFM micrographs demonstrates that the processing of the membranes by IR radiation makes their surface rougher, while the size of pores changes slightly. The permeability of the membranes in various media is measured. More... »

PAGES

880-890

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0965545x17060104

DOI

http://dx.doi.org/10.1134/s0965545x17060104

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1101320546


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