Inelastic deformation of glassy polyaryleneetherketone: Energy accumulation and deformation mechanism View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-01

AUTHORS

O. B. Salamatina, S. N. Rudnev, V. V. Shaposhnikova, A. P. Krasnov, V. Afonicheva, S. N. Salazkin, E. F. Oleinik

ABSTRACT

The plastic deformation of glassy non-annealed polyaryleneetherketone (PAEK) was investigated via deformation calorimetry and thermally stimulated recovery of residual strain. Polymer samples were deformed at room temperature under uniaxial compression up to εdef =–(40−50)% at a rate of 0.04 min−1. It was found that PAEK behaves in the deformation process similarly to many other glassy polymers: It stores internal energy excess at loading and contains two types of different inelastic strain carriers, namely the delayed elastic (εde) and plastic (εpl) strain carriers. The maximum level of the accumulated energy in PAEK reaches ≈ 8.3 J/g, which is close to those for glassy polystyrene and polycarbonate. Nearly all the deformation energy stored in PAEK is carried by the delayed-elastic strain. The carriers of plastic strain carry no extra energy or a very small amount of it. The inelastic deformation of glassy PAEK proceeds in two stages. The carriers of εde are nucleated at the first stage of the deformation process, and the carriers of εpl are nucleated at the second stage. It was shown that, during glassy-polymer loading, the molecular level structures carrying εpl never appear by themselves, but appear only as a result of spontaneous reorganization of εde. In other words, the plastic deformation appears in PAEK owing to the two-step process. This situation is typical for all glassy polymers. More... »

PAGES

18-32

References to SciGraph publications

Journal

TITLE

Polymer Science, Series A

ISSUE

1

VOLUME

58

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0965545x16010107

DOI

http://dx.doi.org/10.1134/s0965545x16010107

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1023930426


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