Macroporous polymeric monoliths as stationary phases in gas adsorption chromatography View Full Text


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Article Info

DATE

2006-08

AUTHORS

A. A. Korolev, V. E. Shiryaeva, T. P. Popova, A. V. Kozin, I. A. D’yachkov, A. A. Kurganov

ABSTRACT

The influence of the conditions of preparation of divinylbenzene-based polymer monoliths on the properties of monolithic capillary columns for use in gas adsorption chromatography was examined. It was found that the polymerization time and the temperature and composition of the polymerization mixture have an effect on the dynamic and chromatographic properties of the columns. The monolithic capillary columns prepared under the optimal synthesis conditions had the height equivalent of a theoretical plate at the level of 20–30 μm, which is an order of magnitude below that of conventional open tubular columns. More... »

PAGES

779-786

References to SciGraph publications

  • 2003-04-26. Monolithic columns for liquid chromatography in ANALYTICAL AND BIOANALYTICAL CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1134/s0965545x06080025

    DOI

    http://dx.doi.org/10.1134/s0965545x06080025

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1000213924


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