Hydrogenation of Polymeric Petroleum Resins in the Presence of Unsupported Sulfide Nanocatalysts View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-12

AUTHORS

N. N. Petrukhina, E. M. Zakharyan, S. A. Korchagina, M. V. Nagieva, A. L. Maksimov

ABSTRACT

Unsupported Ni–Mo and Ni–W sulfide catalysts for the hydrogenation of polymeric petroleum resins are ex situ in a hydrocarbon solvent by the decomposition of oil-soluble bimetallic precursors. It is shown that the activity of the nanocatalysts is higher than that of conventional supported catalysts. The Mo: Ni ratio (1.5: 1) provides the maximum conversion of aromatic and unsaturated moieties of the substrate molecule. It is found that an increase in the process temperature and pressure leads to intensification of polymer chain degradation reactions. The highest degree of hydrogenation is achieved in polymeric petroleum resin solutions with a concentration of 40 wt %; further increase in concentration contributes to the inhibition of thermal degradation reactions. It is shown that the catalyst can be reused without any loss of activity; in addition, the degree of sulfiding of the active phase remains unchanged and the particles do not undergo agglomeration. More... »

PAGES

1295-1303

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0965544117140080

DOI

http://dx.doi.org/10.1134/s0965544117140080

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1101303207


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