Naphthalene hydrogenation over nickel–tungsten sulfide catalysts synthesized in situ from DMSO–hydrocarbon medium emulsions View Full Text


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Article Info

DATE

2017-01

AUTHORS

I. A. Sizova, S. V. Antonov, S. I. Serdyukov, A. L. Maksimov

ABSTRACT

A method for synthesizing unsupported nickel–tungsten sulfide hydrodearomatization catalysts by breaking SPAN-80 surfactant-stabilized nonaqueous emulsions of solutions of different precursors in dimethyl sulfoxide (DMSO) in situ in a hydrocarbon medium has been first studied using ammonium thiotungstate (NH4)2WS4 and 1-butyl-1-methylpiperidinium nickel thiotungstate [BMPip]2Ni[WS4]2 as precursors and nickel nitrate hexahydrate as a nickel source. The synthesized nickel–tungsten catalysts have been characterized by TEM and XPS. The catalytic activity of the in situ synthesized Ni–W particles in naphthalene hydrogenation has been studied at temperatures of 350–400°C and a hydrogen pressure of 5.0 MPa. More... »

PAGES

66-70

References to SciGraph publications

  • 2005-01. Nickel-Molybdenum-Tungsten Sulfide catalysts prepared by in situ activation of tri-metallic (Ni-Mo-W) alkylthiomolybdotungstates in CATALYSIS LETTERS
  • 2016-01-24. Synthesis of nickel–tungsten sulfide hydrodearomatization catalysts by the decomposition of oil-soluble precursors in PETROLEUM CHEMISTRY
  • 2015-01-08. Nickel-tungsten sulfide polyaromatic hydrocarbon hydrogenation nanocatalysts prepared in an ionic liquid in PETROLEUM CHEMISTRY
  • 2003-09. Comparative Study of WS2 and Co(Ni)/WS2 HDS Catalysts Prepared by ex situ/in situ Activation of Ammonium Thiotungstate in CATALYSIS LETTERS
  • 2016-02. Preparation of Ni—W aromatic hydrocarbon hydrogenation catalysts by breaking reverse emulsions or suspensions of a precursor in hydrocarbon feedstock in PETROLEUM CHEMISTRY
  • 2016-06. Nanoheterogeneous catalysis: Definition, state, and research prospects (Review) in PETROLEUM CHEMISTRY
  • 2016-12. Synthesis of Ni–W aromatic hydrocarbon hydrogenation catalysts by the ex situ and in situ decomposition of a precursor based on a dendrimer network in PETROLEUM CHEMISTRY
  • 2011-01. Nanoheterogeneous catalysis: A new sector of nanotechnologies in chemistry and petroleum chemistry (A review) in PETROLEUM CHEMISTRY
  • 2014-09-13. Synthesis and properties of nanosized systems as efficient catalysts for hydroconversion of heavy petroleum feedstock in PETROLEUM CHEMISTRY
  • 2003-03. Cobalt-Molybdenum Sulfide Catalysts Prepared by In Situ Activation of Bimetallic (Co-Mo) Alkylthiomolybdates in CATALYSIS LETTERS
  • Identifiers

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    http://scigraph.springernature.com/pub.10.1134/s0965544117010121

    DOI

    http://dx.doi.org/10.1134/s0965544117010121

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1083751997


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