Cellulose composite membranes for nanofiltration of aprotic solvents View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-11

AUTHORS

T. S. Anokhina, A. A. Yushkin, I. S. Makarov, V. Ya. Ignatenko, A. V. Kostyuk, S. V. Antonov, A. V. Volkov

ABSTRACT

Cellulose composite membranes have been fabricated by casting a cellulose solution in N-methylmorpholine oxide on a nonwoven polyester support. The membranes have been tested for nanofiltration of aprotic solvents. The solvent permeability has changed from 0.11 ± 0.02 to 2.5 ± 0.4 kg/(m2 h bar) in the following order: DMSO > NMP > DMFA > THF > acetone, which can be attributed to a decrease in viscosity of the fluids. The rejection of the anionic dyes Orange II (MW 350) and Remazol Brilliant Blue R (MW 626) has been found to range within 15–85% and 42–94%, respectively, on the solvent nature. Sorption experiments have revealed a noticeable difference between certain solvents in interaction with the membrane material: a lower degree of cellulose swelling in THF (37%) and a higher degree in DMSO (230%). In addition, it has been found that the rejection of solutes by the composite membranes correlates with the degree of cellulose swelling. A rejection of ≥90% has been achieved for Remazol Brilliant Blue R, which has the larger molecule, at a cellulose swelling ratio of 100% or higher. Thus, it has been concluded that polymer swelling leads to narrowing the porous structure of the cellulose layer of the composite membrane and, hence, improvement in separation parameters. More... »

PAGES

1085-1092

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0965544116110025

DOI

http://dx.doi.org/10.1134/s0965544116110025

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1083760920


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