Synthesis of hafnium carbide by mechanochemistry and irradiation View Full Text


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Article Info

DATE

2017-08

AUTHORS

T. F. Grigoreva, B. P. Tolochko, P. V. Logachev, A. I. Ancharov, S. V. Vosmerikov, E. T. Devyatkina, T. A. Udalova, I. A. Vorsina, E. A. Pastukhov, N. Z. Lyakhov

ABSTRACT

The interaction in the Hf–C system during mechanical activation performed in a high-energy planetary ball mill and the irradiation-assisted fabrication of hafnium carbide from an Hf/C mechanocomposite are studied by synchrotron X-ray diffraction (at a quantum energy of 33.7 keV) and high-resolution scanning electron microscopy. The mechanochemical interaction results in the formation of an Hf/C mechanocomposite at the first stage and mechanical activation for ≥8 min forms hafnium carbide. The irradiation of the Hf/C mechanocomposite with a high-energy electron beam (~150 W/mm2) causes melting and spreading of hafnium over the carbon particle surface and the crystallization of hafnium carbide. More... »

PAGES

660-663

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036029517080079

DOI

http://dx.doi.org/10.1134/s0036029517080079

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1095860557


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167 schema:name Budker Institute of Nuclear Physics, Siberian Branch, Russian Academy of Sciences, pr. Akademika Lavrent’eva 11, 630090, Novosibirsk, Russia
168 Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch, Russian Academy of Sciences, ul. Kutateladze 18, 630128, Novosibirsk, Russia
169 Novosibirsk State University, ul. Pirogova 2, 630090, Novosibirsk, Russia
170 rdf:type schema:Organization
171 grid-institutes:grid.465367.5 schema:alternateName Institute of Metallurgy, Ural Branch, Russian Academy of Sciences, ul. Amundsena 101, 620016, Yekaterinburg, Russia
172 schema:name Institute of Metallurgy, Ural Branch, Russian Academy of Sciences, ul. Amundsena 101, 620016, Yekaterinburg, Russia
173 rdf:type schema:Organization
 




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